Force Tensiometer – Sigma 700 / 701

UK based Dyne Testing offer Sigma 700 and 701 force tensiometers that are a powerful and accurate technique to measure static surface and interfacial tension of liquids. These direct measurements allow determination of a number of material and surface properties, such as dynamic contact angle, surface free energy, critical micelle concentration (CMC) and wettability. This information can be used to determine adhesion, absorption, adsorption, cleanliness, surface heterogeneity, density, spreading, porosity, powder or sedimentation wettability, material solubility, biocompatibility and lubricity of solid surfaces, to name but a few.
Sigma force tensiometers are widely used in research, quality control and process control for the determination of:
·          Surface tension
·          Interfacial tension
·          Critical micelle concentration
·          Powder wettability
·          Dynamic contact angle
·          Sedimentation wettability
·          Surface free energy
·          Absorption
·          Cleanliness
·          Surface heterogeneity
Density force tensiometry has become the method of choice for many industrial standards related to characterization of liquids.  It is also the most widely used technique for measuring critical micelle concentration (CMC) of surfactants. In addition, it is the only method to determine the absorption and contact angle of a packed powder or of fibre beds using the Washburn method. The wetting of textiles and individual fibres can also be studied with Sigma force tensiometers.
Measurement principle
When a liquid touches the surface of a solid, the liquid tends to be drawn up in a meniscus. The force exerted by the meniscus is measured and analyzed to determine surface tension. Using high surface free energy probes such as a platinum Du Noüy ring or Wilhelmy plate allow precise measurement of these forces. All Sigma force tensiometers measure surface and interfacial tension using plates or push and pull modes by ring. Correction calculations for rings are made using models from Huh and Mason (Harkins and Jordan, Zuidema & Waters and others also available).Sigma 700/701 force tensiometers come with the OneAttension software for unparalleled performance and usability:
  • Fully automatic measurements avoids user dependant variation and saves time
  • Select readymade experiment recipes or create custom programs for quick and repeatable operations
  • Programmable probe and sample immersion and withdrawal cycle(s)
  • Step by step powder protocol for simple powder wettability measurement
  • Fully automatic CMC measurement

OneAttension is an all-inclusive software enabling immediate access to all measurement capabilities with no need to purchase and install separate software modules. It features an intuitive user interface, live analysis, configurable user groups and accounts and a preset liquid database. Any datapoints or groups of datapoints can be selected, transformed, plotted and analyzed. Data can easily be exported. In-depth analysis is now just a matter of seconds. Accessory modules for dispensers and temperature or pH control can be easily mounted into the measuring unit. In addition, special probes are available for density, wettability and tensiometry measurements as well as holders for fiber and plate studies. Two dispensers can be used simultaneously for critical micelle concentration (CMC) measurements, allowing a full CMC curve to be obtained in one measurement. 

 

Sigma 700

The Sigma 700 has a wide weight range and microbalance maximum load of 210g, which makes it  well suited for dynamic contact angle measurements of large and heavy solid and powder samples.

Sigma 701

Sigma 701 is also a multipurpose tensiometer but equipped with a different microbalance  – 5g optimized for a different range of applications. Sigma 701 can measure in a much more narrow weight range but with improved sensitivity, optimized for fiber measurements.

Software modules for both models are independent and can be acquired separately, giving you the flexibility to customize the instrument to your needs. Modules are available for the following measurements: surface and interfacial tension, dynamic contact angle, CMC, density, powder wettability and sedimentation.

 

 

          Sigma 700          Sigma 701
Available Measurements
Surface tension          Yes          Yes
Interfacial tension          Yes          Yes
Critical micelle concentration          Automatic          Automatic
Dynamic contact angle          Yes          Yes
Surface free energy          Yes          Yes
Powder wettability          Yes          Yes
Density          Yes          Yes
Technical Specifications
Measuring range (mN/m)          1 …2000          1 …1000
Displayed resolution (mN/m)          0.001          0.001
Density range (g/cm³)          0…2.2          0…2.2
Maximum load (g)          210          5
Weighing resolution (mg)          0.01          0.005
Contact angle range          0 …180°          0 …180°
Contact angle resolution          0.01°          0.01°
Calibration & locking          Automatic          Manual
Sample state          Motorised          Motorised
Temperature range (°C)          -20 … +200          -20 … +200

Recommended system requirements

1GHz processor, 1GB MB RAM, 40 GB hard disk drive (20GB free), 1 USB port.

Accessories such as water bath and liquid dispenser may require a free RS-232 port.

Operating system requirements

Windows 7 & 8 (32 or 64 bit), Windows Vista (32 bit), Windows XP SP3 (32 bit).

 

Enquire

Order CodeDescription
40-Sigma 700Sigma 700 Tensiometer, 240VAC, 50 Hz Including:

  • Motorised sample stage
  • Automatic calibration and locking
40-Sigma 701Sigma 701 Tensiometer, 240VAC, 50 Hz Including:

  • Motorised sample stage
  • Automatic calibration and locking

 

 

Enquire

 

 

For accessory details please refer to the list below or contact our Sales Team for assistance.

Order Code     Description
Environment and Sample Control: Temperature, pH, Stirrer & Cabinet
40-T705     Thermostatic vessel (from -10 to +100ºC)
40-T705A     Thermostatic vessel (from -10 to +200ºC)
40-T115     Gas phase temperature controller
40-T708     Temperature probe
40-T102MC     Bath/circulator, Julabo F12-MA
40-T102ME     Bath/circulator, Julabo F25-MA
40-T102MT     Temperature probe for the Julabo bath circulator F25Me
40-T102ED     Bath/circulator, Julabo F12-ED
40-T140CAB     Cabinet
40-T706     Magnetic stirrer
40-T118     pH meter
Critical Micelle Concentration
40-T101     Liquid dispenser, Schott titronic universal 20ml
40-T101A     Cable to connect two T101 dispensers
Powder Wettability
40-T112     Powder wettability measuring device, glass
40-T112A     Powder wettability measuring device, steel Sigma 700 only
40-T112B     Filter paper for T112A, 100 pcs/bag
Density
40-T113     Density measuring device
Sedimentation
40-T119     Sedimentation measuring device
Probes and Calibration
40-T106     Platinum Du Nouy ring
40-T106A     Certificate for Du Nouy ring dimensions
40-T106B     MIKES calibration certificate for Du Nouy ring
40-T107     Wilhelmy Plate, platinum plate with micro roughened surface
40-T107A     Certificate for Wilhelmy plate dimensions
40-T107C     MIKES calibration certificate for Wilhelmy plate
40-T110     Platinum rod
40-T117B     Certified calibration kit
40-T120     Calibration weight
40-T108     Ring re-form tool
Sample Holders
40-T109RF     Sample holder for plates
40-T111     Sample holders for fibres
Vessels
40-T104     Sample vessel, diameter 70mm, 5 pcs/box
40-T105     Sample vessel, diameter 50mm, 5 pcs/box
Computer
40-T130     Computer with pre-installed OneAttension Software
Maintenance & Services
40-STUP-EU     Start up & training
40-1A-UG     OneAttension upgrade
40-SERV1     Service contract level 1
40-SERV2     Service contract level 2
40-SERV3     Extended warranty

 

For a detailed list of accessories please refer to the attachment

  Sigma 700-701-Accessory List